4-(3-Chlorophenyl)-1-(3-chloropropyl)piperazin-1-ium chloride redetermined at 100 K
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چکیده
منابع مشابه
3-Fluorobenzoic acid–4-acetylpyridine (1/1) at 100 K
In the title compound, C(7)H(5)FO(2)·C(7)H(7)NO, a moderate-strength hydrogen bond is formed between the carboxyl group of one mol-ecule and the pyridine N atom of the other. The benzoic acid mol-ecule is observed to be disordered over two positions with the second orientation only 4% occupied. This disorder is also reflected in the presence of diffuse scattering in the diffraction pattern.
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The title compound, C(9)H(8)N(3)O(+)·Cl(-), was isolated from a liquid culture of streptomyces sp. In the cation, the ring system makes a dihedral angle of 0.2 (2)° with the amide group. The protonation creating the cation occurs at ome of the N atoms in the quinoxaline ring system. In the crystal, the ions are linked through N-H⋯O and N-H⋯Cl hydrogen bonds, forming a two-dimensional network pa...
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In the cation of the title compound, C(5)H(8)N(3) (+)·Cl(-), the C-N(H(2)) bond distance [1.348 (3) Å] is at the lower end of the range for aryl amines. In the crystal structure, cations and anions are linked via N-H⋯Cl hydrogen bonds, forming one-dimensional chains along [100].
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In the title compound, C10H10Cl2N2OS, the mol-ecule adopts a trans-cis conformation with respect to the position of the carbonyl group and the chloro-phenyl groups relative to the thiono group across the C-N bonds. The mol-ecule is stabilized by an N-H⋯O hydrogen bond. In the crystal, mol-ecules are linked by N-H⋯S and C-H⋯O hydrogen bonds, forming zigzag chains along the b-axis direction. C-H⋯...
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In the cation of the title salt, C(11)H(12)IN(4) (+)·Cl(-), the two aromatic rings are oriented to each other at 9.3 (2)°. In the crystal, the two independent Cl(-) anions lie on twofold rotation axes. N-H⋯Cl hydrogen bonds between the cations and anions generate a supra-molecular layer parallel to (010).
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ژورنال
عنوان ژورنال: IUCrData
سال: 2016
ISSN: 2414-3146
DOI: 10.1107/s2414314616001681